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Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
- Author:
- George H. Stout
- Publisher:
- Wiley-Interscience
- Publication Date:
- April 24, 1989
- Number of pages:
- 480 pages
- Language:
- English
- Binding:
- Hardcover
- ISBN-10:
- 0471607118
- ISBN-13:
- 9780471607113